Turkish Journal of Chemistry
Abstract
In the present work, a facile hydrothermal route was employed to synthesize the nanocomposite MgFe2O4/MoS2, which acted as a heterogeneous photo-Fenton catalyst for the degradation of a synthetic diazo dye, Acid Blue 113 (AB113). The nanocatalyst produced underwent analysis using multiple characterization techniques. The parameters influencing the oxidative reaction were statistically modeled and optimized using response surface methodology. Optimal degradation efficiency for AB113 (94.92%) was attained at pH 8.79 using 10 mg of MgFe2O4/MoS2 nanocatalyst, 1.6 mL of H2O2, and a reaction duration of 27 min. The synergistic effect resulting from the formation of electron-hole pairs renders the combined photocatalysis and Fenton process a more efficient treatment approach. The kinetic study data indicate that the photo-Fenton process follows the pseudo-first-order model. The nanocatalyst fabricated demonstrated exceptional stability, maintaining a high degradation performance after seven consecutive photo-Fenton cycles. The results obtained indicate that the MgFe2O4.MoS2/H2O2/Vis system is an effective method for treating wastewaters containing organic contaminants.
Author ORCID Identifier
ZAHRA ZEINALI: 0009-0000-7017-0628
LEILA ERSHADI AFSHAR: 0009-0003-4863-4563
NAZ CHAIBAKHSH: 0000-0001-8545-1449
FARNAZ ISAPOUR: 0009-0003-5284-0140
DOI
10.55730/1300-0527.3796
Keywords
Acid Blue 113, azo dye degradation, MgFe2O4/MoS2 nanocomposite, optimization, photo-Fenton
First Page
259
Last Page
270
Publisher
The Scientific and Technological Research Council of Türkiye (TÜBİTAK)
Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.
Recommended Citation
ZEINALI, Z, ERSHADI AFSHAR, L, CHAIBAKHSH, N, & ISAPOUR, F (2026). Efficient heterogeneous photo-Fenton degradation of azo dyes using the nanocomposite MgFe2O4/MoS2. Turkish Journal of Chemistry 50 (3): 259-270. https://doi.org/10.55730/1300-0527.3796