The Mechanism and Crystal Structure of 2-Methoxy-2-methyl-4-phenyl-3,4,4a, 10b-tetrahydro-2H,5H-pyrano[3,2-c]chromen-5-one. Acetal of Warfarin Acid

Authors

SAIRA SHAHZADI
SAQIB ALI
IRUM ASIF
RIZWANA ASHRAF
GUO-XIN JIN

DOI

-

Abstract

Acetal of warfarin acid has been synthesized via a hemi acetal intermediate and structurally characterized by X-ray diffraction. The crystal structure shows that the title compound was formed by the hydrolysis of warfarin acid in methanol at pH 3, with space group P2_1/n and unit cell parameters a = 5.859 (17), b =16.745 (5), c = 16.402 (5) Å, \alpha = 90.00; \beta = 94.853 (4), and \gamma = 90.00°.

Keywords

Warfarin acid, synthesis, acetal, crystal structure

First Page

703

Last Page

709

Recommended Citation

SHAHZADI, SAIRA; ALI, SAQIB; ASIF, IRUM; ASHRAF, RIZWANA; and JIN, GUO-XIN (2006) "The Mechanism and Crystal Structure of 2-Methoxy-2-methyl-4-phenyl-3,4,4a, 10b-tetrahydro-2H,5H-pyrano[3,2-c]chromen-5-one. Acetal of Warfarin Acid," Turkish Journal of Chemistry: Vol. 30: No. 6, Article 6. Available at: https://journals.tubitak.gov.tr/chem/vol30/iss6/6